xrd标准图谱分析

问题描述:

xrd标准图谱分析
PDF#09-0413: QM=Star(+); d=(Unknown); I=Diffractometer
Mayenite, syn
Ca12 Al14 O33 (Colorless)
Radiation=CuKa1 Lambda=1.54056 Filter=Ni
Calibration= d-Cutoff= I/Ic(RIR)=
Ref= Natl. Bur. Stand. (U.S.), Circ. 539, 9 20 (1960)
Cubic - Powder Diffraction,I-43d (220) Z=2 mp=
Cell=11.982 Pearson=cI118 (?)
Density(c)=2.676 Density(m)=3.16A Mwt=1386.68 Vol=1720.24 F(30)=50.9(.0159,37)
Ref= Ibid.
Strong Line: 2.68/X 4.89/X 2.45/5 3.00/5 2.19/4 1.95/3 1.66/3 1.60/3 3.20/3 2.56/2
NOTE:Sample prepared by Portland Cement Association Fellowship at NBS, Gaithersburg, Maryland, USA.
Spectrographic analysis showed the following impurities: 0.1-1.0% each of Na, Si, Sr; 0.01-0.1% Fe, Mg; 0.001-0.01% each of Cu, Mn, Mo.
Pattern taken at 25 C.
See ICSD 6287 (PDF 01-070-2144); See ICSD 62040 (PDF 01-078-0910).
d(A) I(f) I(v) hkln^22-Theta Theta1/(2d) 2pi/d
4.890 95.0 52.0 2116 18.126 9.0630.10221.2849
4.2406.04.0 2208 20.93410.4670.11791.4819
3.790 16.0 11.0 310 10 23.45311.7260.13191.6578
3.204 25.0 21.0 321 14 27.82213.9110.15611.9610
2.998 45.0 40.0 400 16 29.77614.8880.16682.0958
2.680100.0100.0 420 20 33.40716.7030.18662.3445
2.556 18.0 19.0 332 22 35.07917.5390.19562.4582
2.447 50.0 55.0 422 24 36.69618.3480.20432.5677
2.350 10.0 11.0 510 26 38.26819.1340.21282.6737
2.189 40.0 49.0 521 30 41.20620.6030.22842.8703
2.054 10.0 13.0 530 34 44.05022.0250.24343.0590
1.945 30.0 41.0 611 38 46.66123.3300.25713.2304
1.8508.0 12.0 541 42 49.21124.6050.27033.3963
1.7676.09.0 631 46 51.68825.8440.28303.5558
1.730 12.0 19.0 444 48 52.87826.4390.28903.6319
1.6958.0 13.0 710 50 54.05827.0290.29503.7069
1.662 30.0 48.0 640 52 55.22227.6110.30083.7805
1.630 10.0 16.0 721 54 56.40228.2010.30673.8547
1.601 30.0 50.0 642 56 57.51828.7590.31233.9245
1.5226.0 11.0 732 62 60.80830.4040.32854.1282
1.4986.0 11.0 800 64 61.88930.9440.33384.1944
1.4758.0 15.0 741 66 62.96331.4820.33904.2598
1.393 18.0 35.0 831 74 67.14133.5710.35894.5105
1.3564.08.0 752 78 69.22934.6150.36874.6336
1.3408.0 16.0 840 80 70.17635.0880.37314.6889
1.3078.0 16.0 842 84 72.22236.1110.38264.8073
1.2926.0 12.0 921 86 73.19536.5980.38704.8631
1.2776.0 13.0 664 88 74.19837.0990.39154.9203
跪求有识之人为我解答,分析下上面是什么意思,其实我最想知道的是衍射角和衍射强度两组数据,请告我那两组是?

这是一张PDF卡片,矿相是水泥(C12A7)
d(A)(晶面间距)
I(f)(衍射峰强度)
I(v) (积分强度)
h k l(晶面指数)
n^2 (晶面指数平方和)
2-Theta(2θ角)
Theta(θ角)
1/(2d)
2pi/d