苯乙烯聚合聚苯乙烯的实验室制法
问题描述：
苯乙烯聚合聚苯乙烯的实验室制法
答
solution polymerization.
Initiated with BPO or AIBN (1wt% or 1mol%)
common solvent: THF or toluene.
temperature: 65-70 (AIBN); 90 (BPO)
time: 24h
precipitate in methanol
filter the solid off and dry at 60C overnight
答
密封小瓶,装1/2苯乙烯
140度,24小时
聚合完成